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A new intersecting tunnel structure in the AIMIII[PO3(OH)]2 series for AI = Ag, MIII = In : Analysis of structural relationships

Identifieur interne : 005A11 ( Main/Repository ); précédent : 005A10; suivant : 005A12

A new intersecting tunnel structure in the AIMIII[PO3(OH)]2 series for AI = Ag, MIII = In : Analysis of structural relationships

Auteurs : RBID : Pascal:09-0134109

Descripteurs français

Pascal (Inist)
- Structure tunnel, Analyse structurale, Indium, Croissance cristalline en solution, Synthèse hydrothermale, Structure cristalline, Groupe espace, Paramètre cristallin, Effet tunnel, Direction cristallographique, Groupe hydroxyle, Spectre IR, Diffraction RX, Argent, Monocristal, In, 8110D, 6166.
Wicri :
- concept : Argent.

English descriptors

KwdEn :
- Channel structure, Crystal growth from solutions, Crystal structure, Crystallographic direction, Hydrothermal synthesis, Hydroxyl group, Indium, Infrared spectra, Lattice parameters, Monocrystals, Silver, Space groups, Structural analysis, Tunnel effect, XRD.

Abstract

A new indium hydroxyphosphate containing silver, AgIn[PO₃(OH)]₂, has been synthesized using hydrothermal method. It crystallizes in the P2₁/c space group with the cell parameters a = 6.6400(2)Å, b=14.6269(6)Å, c=6.6616(4)A, β=95.681(5)°, V=643.82(6)Å³, Z=4. Its three-dimensional framework, built up of comer-sharing PO₃(OH) tetrahedra and InO₆ octahedra, presents intersecting tunnels running along <111> and [100] directions, in which the Ag⁺ cations are located. The presence of hydroxyl groups has been confirmed from IR spectroscopy studies and hydrogen atoms were located from the single crystal X-ray diffraction study. The structural relationships with the other compounds of general formula A^IM^III[PO₃(OH)]₂ are analyzed.

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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">A new intersecting tunnel structure in the A<sup>I</sup>
M<sup>III</sup>
[PO<sub>3</sub>
(OH)]<sub>2</sub>
 series for A<sup>I</sup>
 = Ag, M<sup>III</sup>
 = In : Analysis of structural relationships</title>
<author><name sortKey="Guesdon, Anne" uniqKey="Guesdon A">Anne Guesdon</name>
<affiliation wicri:level="4"><inist:fA14 i1="01"><s1>Laboratoire CRISMAT, UMR 6508 CNRS ENSICAEN, Université de Caen Basse-Normandie, 6 Boulevard du Maréchal juin</s1>
<s2>14050 Caen</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
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<sZ>4 aut.</sZ>
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<country>France</country>
<placeName><region type="region" nuts="2">Basse-Normandie</region>
<settlement type="city">Caen</settlement>
</placeName>
<orgName type="university">Université de Caen Basse-Normandie</orgName>
</affiliation>
</author>
<author><name sortKey="Romero Sarria, Francesca" uniqKey="Romero Sarria F">Francesca Romero Sarria</name>
<affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Laboratoire Catalyse et Spectrochimie, UMR 6506 CNRS ENSICAEN, 6 Boulevard Maréchal juin</s1>
<s2>14050 Caen</s2>
<s3>FRA</s3>
<sZ>2 aut.</sZ>
</inist:fA14>
<country>France</country>
<placeName><region type="region" nuts="2">Basse-Normandie</region>
<settlement type="city">Caen</settlement>
</placeName>
</affiliation>
</author>
<author><name sortKey="Tenailleau, Christophe" uniqKey="Tenailleau C">Christophe Tenailleau</name>
<affiliation wicri:level="4"><inist:fA14 i1="01"><s1>Laboratoire CRISMAT, UMR 6508 CNRS ENSICAEN, Université de Caen Basse-Normandie, 6 Boulevard du Maréchal juin</s1>
<s2>14050 Caen</s2>
<s3>FRA</s3>
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<orgName type="university">Université de Caen Basse-Normandie</orgName>
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</author>
<author><name sortKey="Raveau, Bernard" uniqKey="Raveau B">Bernard Raveau</name>
<affiliation wicri:level="4"><inist:fA14 i1="01"><s1>Laboratoire CRISMAT, UMR 6508 CNRS ENSICAEN, Université de Caen Basse-Normandie, 6 Boulevard du Maréchal juin</s1>
<s2>14050 Caen</s2>
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<country>France</country>
<placeName><region type="region" nuts="2">Basse-Normandie</region>
<settlement type="city">Caen</settlement>
</placeName>
<orgName type="university">Université de Caen Basse-Normandie</orgName>
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<date when="2009">2009</date>
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<seriesStmt><idno type="ISSN">1293-2558</idno>
<title level="j" type="abbreviated">Solid state sci.</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Channel structure</term>
<term>Crystal growth from solutions</term>
<term>Crystal structure</term>
<term>Crystallographic direction</term>
<term>Hydrothermal synthesis</term>
<term>Hydroxyl group</term>
<term>Indium</term>
<term>Infrared spectra</term>
<term>Lattice parameters</term>
<term>Monocrystals</term>
<term>Silver</term>
<term>Space groups</term>
<term>Structural analysis</term>
<term>Tunnel effect</term>
<term>XRD</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Structure tunnel</term>
<term>Analyse structurale</term>
<term>Indium</term>
<term>Croissance cristalline en solution</term>
<term>Synthèse hydrothermale</term>
<term>Structure cristalline</term>
<term>Groupe espace</term>
<term>Paramètre cristallin</term>
<term>Effet tunnel</term>
<term>Direction cristallographique</term>
<term>Groupe hydroxyle</term>
<term>Spectre IR</term>
<term>Diffraction RX</term>
<term>Argent</term>
<term>Monocristal</term>
<term>In</term>
<term>8110D</term>
<term>6166</term>
</keywords>
<keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Argent</term>
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<front><div type="abstract" xml:lang="en">A new indium hydroxyphosphate containing silver, AgIn[PO<sub>3</sub>
(OH)]<sub>2</sub>
, has been synthesized using hydrothermal method. It crystallizes in the P2<sub>1</sub>
/c space group with the cell parameters a = 6.6400(2)Å, b=14.6269(6)Å, c=6.6616(4)A, β=95.681(5)°, V=643.82(6)Å<sup>3</sup>
, Z=4. Its three-dimensional framework, built up of comer-sharing PO<sub>3</sub>
(OH) tetrahedra and InO<sub>6</sub>
 octahedra, presents intersecting tunnels running along <111> and [100] directions, in which the Ag<sup>+</sup>
 cations are located. The presence of hydroxyl groups has been confirmed from IR spectroscopy studies and hydrogen atoms were located from the single crystal X-ray diffraction study. The structural relationships with the other compounds of general formula A<sup>I</sup>
M<sup>III</sup>
[PO<sub>3</sub>
(OH)]<sub>2</sub>
 are analyzed.</div>
</front>
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<fA08 i1="01" i2="1" l="ENG"><s1>A new intersecting tunnel structure in the A<sup>I</sup>
M<sup>III</sup>
[PO<sub>3</sub>
(OH)]<sub>2</sub>
 series for A<sup>I</sup>
 = Ag, M<sup>III</sup>
 = In : Analysis of structural relationships</s1>
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<fA11 i1="01" i2="1"><s1>GUESDON (Anne)</s1>
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<fA11 i1="02" i2="1"><s1>ROMERO SARRIA (Francesca)</s1>
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<s3>FRA</s3>
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<s3>FRA</s3>
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<fC01 i1="01" l="ENG"><s0>A new indium hydroxyphosphate containing silver, AgIn[PO<sub>3</sub>
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/c space group with the cell parameters a = 6.6400(2)Å, b=14.6269(6)Å, c=6.6616(4)A, β=95.681(5)°, V=643.82(6)Å<sup>3</sup>
, Z=4. Its three-dimensional framework, built up of comer-sharing PO<sub>3</sub>
(OH) tetrahedra and InO<sub>6</sub>
 octahedra, presents intersecting tunnels running along <111> and [100] directions, in which the Ag<sup>+</sup>
 cations are located. The presence of hydroxyl groups has been confirmed from IR spectroscopy studies and hydrogen atoms were located from the single crystal X-ray diffraction study. The structural relationships with the other compounds of general formula A<sup>I</sup>
M<sup>III</sup>
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A new intersecting tunnel structure in the AIMIII[PO3(OH)]2 series for AI = Ag, MIII = In : Analysis of structural relationships

A new intersecting tunnel structure in the AIMIII[PO3(OH)]2 series for AI = Ag, MIII = In : Analysis of structural relationships

Descripteurs français

English descriptors

Abstract

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Le document en format XML

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